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Quantification of Hydrogen Concentrations in Surface and Interface Layers and Bulk Materials through Depth Profiling with Nuclear Reaction Analysis
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JoVE Journal Ingegneria
Quantification of Hydrogen Concentrations in Surface and Interface Layers and Bulk Materials through Depth Profiling with Nuclear Reaction Analysis
DOI:

14:11 min

March 29, 2016

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Capitoli

  • 00:05Titolo
  • 01:29Single Crystal Surface Preparation for Nuclear Reaction Analysis (NRA) in Ultra-high Vacuum
  • 08:07Surface Hydrogen Nuclear Reaction Analysis Measurements
  • 09:24Bulk and Interface Hydrogen Nuclear Reaction Analysis: Preparation and Measurement
  • 11:02Results: Nuclear Reaction Analysis Hydrogen Depth Profiles for Single Crystal Palladium and from Silicon Dioxide Films on Silicon
  • 12:50Conclusion

Summary

Traduzione automatica

We illustrate the application of 1H(15N,αγ)12C resonant nuclear reaction analysis (NRA) to quantitatively evaluate the density of hydrogen atoms on the surface, in the volume, and at an interfacial layer of solid materials. The near-surface hydrogen depth profiling of a Pd(110) single crystal and of SiO2/Si(100) stacks is described.

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