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HKUST-1 as a Heterogeneous Catalyst for the Synthesis of Vanillin
 

HKUST-1 as a Heterogeneous Catalyst for the Synthesis of Vanillin

Article DOI: 10.3791/54054-v • 11:15 min • July 23rd, 2016
July 23rd, 2016 •
1, 1, 1, 2, 3, 4, 5, 5, 1
1Autonomous Metropolitan University-Azcapotzalco, 2Institute of Catalysis and Petroleum Chemistry, ICP-CSIC, 3Department of Chemistry, Autonomous Metropolitan University-Iztapalapa, 4Department of Chemistry, Center of Investigation and Superior Studies (IPN), 5Research Institute of Material, National Autonomous University of Mexico

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The conversion of trans-ferulic acid to vanillin was achieved by heterogeneous catalysis. HKUST-1 was employed in this synthesis and the essential step in the catalytic process was the generation of unsaturated metal sites. Thus, when the catalyst was activated under vacuum, full vanillin conversion (yield of 95%) was obtained.

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HKUST-1 Heterogeneous Catalyst Synthesis Vanillin Trans Ferulic Acid Porous Coordination Polymer Unsaturated Metal Sites Catalytic Process Flavoring Agent Mild Oxidation Conditions Experimental Protocol Activation Of HKUST-1 Rebeca Yepez Graduate Student Crystallinity Powder X-ray Diffraction Pattern Dissolvation Activation System
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