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Preparation of SNS Cobalt(II) Pincer Model Complexes of Liver Alcohol Dehydrogenase
 

Preparation of SNS Cobalt(II) Pincer Model Complexes of Liver Alcohol Dehydrogenase

Article DOI: 10.3791/60668-v • 06:31 min • March 19th, 2020
March 19th, 2020 •
1, 2, 2, 1, 1, 1, 1, 1
1Department of Chemistry and Biochemistry, Fairfield University, 2Department of Chemistry, Keene State College

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The preparation of SNS pincer cobalt(II) model complexes of liver alcohol dehydrogenase is presented here. The complexes can be prepared by reacting the ligand precursor with CoCl2·6H2O and can then be recrystallized by allowing diethyl ether to slowly diffuse into an acetonitrile solution that contains the cobalt complex.

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Preparation SNS Cobalt(II) Pincer Model Complexes Liver Alcohol Dehydrogenase Single Crystals Complex Formation Recrystallization Method Coordination Complexes Inorganic Coordination Compounds Acetonitrile Solution Concentrated 2 6-BIS-N-isopropyl-N'methyleneimidzole-2-thione-pyridine Cobalt II Chloride Hexahydrate Round Bottom Flask Emerald Green Color Reflux Stir Rotovap Reduced Pressure Chloro-N3-S S N-2 Tetrachlorocobaltate Recrystallization Slow Vapor Diffusion
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