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Calibration Procedures for Orthogonal Superposition Rheology
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Calibration Procedures for Orthogonal Superposition Rheology

Calibration Procedures for Orthogonal Superposition Rheology

DOI:
10.3791/61965-v

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08:43 min

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November 18, 2020

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,
1Material Measurement Laboratory,National Institute of Standards and Technology, 2Department of Chemical Engineering,Texas Tech University

Capitoli

  • 00:04Introduction
  • 00:57Rheometer Setup
  • 02:17Test Material Loading
  • 03:38Viscosity Calibration Measurement and Verification
  • 06:02Results: Representative Steady-Shear Sweep and Orthogonal Frequency Sweep Testing and Analysis
  • 07:56Conclusion

Summary

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We present a detailed calibration protocol for a commercial orthogonal superposition rheology technique using Newtonian fluids including end-effect correction factor determination methods and recommendations for best practices to reduce experimental error.

Tags

Orthogonal Superposition RheologyCalibration ProceduresMeasurement ErrorEnd Effect FactorsTemperature MeasurementEnvironmental ControlGeometry AssemblyTransducer ZeroingSample Loading

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