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微波辅助分子内Diels-Alder反应的功能化萘/变色染料的合成脱氢

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Microwave-assisted Intramolecular Dehydrogenative Diels-Alder Reactions for the Synthesis of Functionalized Naphthalenes/Solvatochromic Dyes

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微波辅助分子内Diels-Alder反应的功能化萘/变色染料的合成脱氢

DOI:

10.3791/50511-v

•

12:07 min

•

April 01, 2013

•

Laura S. Kocsis, Erica Benedetti, Kay M. Brummond

¹Department of Chemistry,University of Pittsburgh

Chapters

00:05Title
02:33Microwave-assisted Dehydrogenative DA Reaction
04:16Palladium-catalyzed Cross-coupling Reaction
07:06Preparation of Dye Solution for Photophysical Studies
07:50Fluorescence Emission Spectroscopy
08:47Results: Synthesis and Photophysical Analysis of Functionalized Nephthalenes/Solvatochromic Fluorescent Dyes
11:10Conclusion

Summary

자동 번역

微波辅助分子内的脱氢的Diels-Alder反应（DA）提供简洁的访问功能化环戊[<em> B</em>]萘积木。一个步骤转换成脱氢DA双环[2.2.2]辛烯酮类化合物的新型溶致变色荧光染料通过布赫瓦尔德-哈特维希钯催化交叉偶联反应证明了这种方法的效用。

Tags

Microwave-assisted Intramolecular Dehydrogenative Diels-Alder Reactions Functionalized Naphthalenes Solvatochromic Dyes Cyclopenta[b]naphthalenes Buchwald-Hartwig Palladium-catalyzed Cross-coupling Fluorescence Spectroscopy

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