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A Protocol for Safe Lithiation Reactions Using Organolithium Reagents

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A Protocol for Safe Lithiation Reactions Using Organolithium Reagents

A Protocol for Safe Lithiation Reactions Using Organolithium Reagents

DOI:

10.3791/54705-v

•

09:45 min

•

November 12, 2016

•

Michael R. Gau, Michael J. Zdilla

¹Department of Chemistry,Temple University

Chapters

00:05Title
00:39Organolithium Handling and Disposal Procedures
02:07Small-scale Lithiation
06:21Lithiation in a Glovebox
08:25Results: Lithiation of tert-Butylamine with tert-Butyllithium
08:54Conclusion

Summary

자동 번역

The safe and proper use of organolithium reagents is described.

Tags

Organolithium Reagents Lithiation Reactions Safety Protocol Pyrophoric Reagents Synthetic Chemistry Quenching Agents Inert Gas Blanket Schlenk Flask Tert-butylamine

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