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Chapters
- 00:04Title
- 02:32Leak Check for all the High Vacuum Vessels and Their Connection to the HVL
- 02:59Dehydroxylated Silica Preparation
- 03:55Solvent Preparation (Removal of Oxygen & Moisture)
- 04:35General Procedure for Grafting Metal Complexes on Dehydroxylated Silica using Hf(NMe2)4
- 06:15Preparation of the Catalyst and Imine Metathesis Catalysis
- 07:29Results: Characterization of New Heterogeneous Catalyst for Imine Metathesis
- 08:58Conclusion
En ny gruppe IV metal katalysator for Lindholm meta tese er udarbejdet af podning Amin metal kompleks på dehydroxyleret silica. Overflade metalfragmenter er karakteriseret ved hjælp af FT-IR, elementær mikroanalyse, og solid-state NMR spektroskopi. Yderligere dynamiske nukleare polariserings overflade forbedrede NMR-spektroskopi-eksperimenter supplerer bestemmelsen af koordinations området.
