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可靠的化学: 整洁和液体辅助球磨机研磨试验的可再生结果协议

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Química

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JoVE Journal Química

Reliable Mechanochemistry: Protocols for Reproducible Outcomes of Neat and Liquid Assisted Ball-mill Grinding Experiments

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可靠的化学: 整洁和液体辅助球磨机研磨试验的可再生结果协议

DOI:

10.3791/56824-v

•

13:05 min

•

January 23, 2018

•

Ana M. Belenguer, Giulio I. Lampronti², Jeremy K. M. Sanders

¹Department of Chemistry,University of Cambridge, ²Department of Earth Sciences,University of Cambridge

Capítulos

00:05Título
00:56Calibration of Electronic Air-Displacement Pipette in Reverse Pipetting Mode
03:04Ball Mill Liquid-Assisted Grinding (LAG) Synthesis of 4-Chlorophenyl-2-nitrophenyl Disulfide (1-2) Using High-Affinity Solvent (17.0 μL Acetone)
06:54Ball Mill LAG Synthesis of 1-2 Using a Low-Affinity Solvent (65 μL Methanol)
09:46Results: Solvent Milling Equilibrium Curves for the Ball Mill LAG Synthesis of Heterodimer 1-2
11:29Conclusion

Summary

Tadução automática

在铣削条件下, 我们给出了在固态系统中, 作为溶剂浓度函数的相组成的实验平衡曲线的详细步骤。

Tags

Mechanochemistry Ball-mill Grinding Liquid-assisted Grinding (LAG)Polymorphism Solvent Effects Experimental Design Reproducibility Pipette Calibration Equilibrium Crystal Phase Composition

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