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合成和Iodoaziridines纯化涉及定量选择最优固定相的色谱

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Química

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JoVE Journal Química

Synthesis and Purification of Iodoaziridines Involving Quantitative Selection of the Optimal Stationary Phase for Chromatography

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合成和Iodoaziridines纯化涉及定量选择最优固定相的色谱

DOI:

10.3791/51633-v

•

10:14 min

•

May 16, 2014

•

Tom Boultwood, Dominic P. Affron, James A. Bull

¹Department of Chemistry,Imperial College London

Capítulos

00:04Título
01:26Preparation of Iodoaziridines with Diiodomethyllithium
04:32Assessment of Product Stability to Stationary Phases for Chromatography
07:04Deactivation of Basic Alumina and Purification of the Iodoaziridine
08:01Results: Diastereoselective Synthesis and Characterization of Iodoaziridines
09:39Conclusion

Summary

Tadução automática

一个协议的非对映选择性一锅准备顺 - N-TS-iodoaziridines描述。的diiodomethyllithium，除了N-TS醛亚胺和氨基宝石 -二碘化中间体iodoaziridines被证实环化生成。还包括的是一种协议通过色谱法快速和定量评估的最合适的固定相进行纯化。

Tags

Keywords: Iodoaziridines Diiodomethyllithium N-Ts Aldimines Diastereoselective Synthesis Column Chromatography Stationary Phase Selection Quantitative Analysis 1H NMR Spectroscopy Basic Alumina Sensitive Compounds

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