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35-吡啶N-氧化物脱水的合成、结晶和光谱表征

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Química

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JoVE Journal Química

Syntheses, Crystallization, and Spectroscopic Characterization of 3,5-Lutidine N-Oxide Dehydrate

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35-吡啶N-氧化物脱水的合成、结晶和光谱表征

DOI:

10.3791/57233-v

•

06:18 min

•

April 24, 2018

•

Rosario Merino-García, Samuel Hernández-Anzaldo, Yasmi Reyes-Ortega

¹Centro de Química, Instituto de Ciencias,Benemérita Universidad Autónoma de Puebla

Capítulos

00:04Título
01:14Reaction
02:19Basicity Adjustment and Extraction
03:17Crystallization Process and Analysis of 3,5-Lutidine N-oxide Dehydrate
04:25Results: Characterization of 3,5-Lutidine N-Oxide Dehydrate
05:51Conclusion

Summary

Tadução automática

在此, 我们报告的合成和结晶的 35-吡啶n-氧化物脱水的一个简单的协议, 不同于经典合成吡啶N氧化物。该协议采用不同的起始材料, 反应时间较少, 产生一种新的溶解超分子结构, 在缓慢蒸发下结晶。

Tags

3 5-lutidine N-oxide Dehydrate Solvated Supramolecular Structure Synthetic Organic Chemistry Inorganic Chemistry 2-aminopyridine-3 5-dicarboxylic Acid Glacial Acetic Acid 3 5-dimethylpyridine Hydrogen Peroxide High-vacuum Distillation Sodium Carbonate Chloroform Sodium Sulfate Diethyl Ether Crystallization

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