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Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles
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JoVE Journal Química
Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles

Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles

DOI:
10.3791/57667-v

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11:54 min

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June 25, 2018

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, , , , , , ,
1Department of Chemical Engineering,Virginia Polytechnic Institute and State University, 2Center for Integrated Nanotechnologies,Los Alamos National Laboratory, 3Advanced Photon Source,Argonne National Laboratory, 4X-ray Science Division,Argonne National Laboratory, 5Environmental Molecular Science Laboratory,Pacific Northwest National Laboratory

Capítulos

  • 00:04Título
  • 00:44Palladium(II) Acetate Recrystallization
  • 03:54Colloidal Pd Nanoparticle Synthesis in Pyridine
  • 06:25Pd Nanoparticle Characterization by Ex Situ Small-Angle X-Ray Scattering (SAXS)
  • 09:52Results: Kinetics of Nucleation and Growth of Pd Nanoparticles in Toluene and Pyridine
  • 11:20Conclusion

Summary

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The main goal of this work is to elucidate the role of capping agents in regulating the size of palladium nanoparticles by combining in situ small angle x-ray scattering (SAXS) and ligand-based kinetic modeling.

Tags

PalladiumNanoparticlesNucleationGrowthSAXSKinetic RatesCapping LigandsColloidalMetal OxidesPalladium AcetateVacuum FiltrationCrystallization

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