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Performing In Situ Closed-Cell Gas Reactions in the Transmission Electron Microscope
 

Performing In Situ Closed-Cell Gas Reactions in the Transmission Electron Microscope

Article DOI: 10.3791/62174-v • 14:21 min • July 24th, 2021
July 24th, 2021 •
1, 1, 2, 3, 4, 4, 1, 5
1Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, 2Protochips Inc., 3Department of Materials Science & Engineering, University of Michigan, 4Catalytic Carbon Transformation & Scale-up, National Renewable Energy Laboratory, 5Materials Science & Technology Division, Oak Ridge National Laboratory

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Here, we present a protocol for performing in situ TEM closed-cell gas reaction experiments while detailing several commonly used sample preparation methods.

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Keywords: In Situ Closed-cell Gas Reaction CCGR Scanning Transmission Electron Microscopy Catalysts Structural Materials Carbon Nanotubes Real-time Analysis Elevated Temperature Atmospheric Pressure Sample Preparation Powder Deposition Colloidal Suspension E-chip Mask
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