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连续流反应器中的可扩展巴尔茨-席曼反应方案
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JoVE Journal Química
A Scalable Balz-Schiemann Reaction Protocol in a Continuous Flow Reactor
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连续流反应器中的可扩展巴尔茨-席曼反应方案

DOI:
10.3791/64937-v

•

05:21 min

•

February 10, 2023

•

, , , , ,
1Shenzhen Hwagen Pharmaceutical Co., Ltd, 2Guangdong Raffles Pharmaceutical Technology Co., Ltd

Capítulos

  • 00:04Introduction
  • 00:46Continuous Flow Equipment Setup, Safety Check, and Leak Test
  • 02:29Continuous Flow Reaction Process
  • 03:29Results: Effect of Temperature and Residence Time on Continuous Flow Reaction
  • 04:33Conclusion

Summary

Tadução automática

Tadução automática

提出了一个详细的可扩展连续流动方案，用于通过Balz-Schiemann反应从芳基胺合成芳基氟化物。

Tags

Balz-Schiemann ReactionContinuous Flow ReactorAryl FluorideAryl AmineFine Chemical IndustryPharmaceutical IndustryMicroflow ReactorDynamic Mixing Tube ReactorTemperature RegulationSafetyLeakage CheckSteady State EquilibriumProduct Collection

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