Journal
/
Engineering
/
Quantification of Hydrogen Concentrations in Surface and Interface Layers and Bulk Materials through Depth Profiling with Nuclear Reaction Analysis
JoVE Journal
Engineering
A subscription to JoVE is required to view this content.  Sign in or start your free trial.
JoVE Journal Engineering
Quantification of Hydrogen Concentrations in Surface and Interface Layers and Bulk Materials through Depth Profiling with Nuclear Reaction Analysis

Quantification of Hydrogen Concentrations in Surface and Interface Layers and Bulk Materials through Depth Profiling with Nuclear Reaction Analysis

DOI:
10.3791/53452-v

•

14:11 min

•

March 29, 2016

•

, , , ,
1Institute of Industrial Science,The University of Tokyo, 2Micro Analysis Laboratory, Tandem accelerator, The University Museum,The University of Tokyo

Chapters

  • 00:05Title
  • 01:29Single Crystal Surface Preparation for Nuclear Reaction Analysis (NRA) in Ultra-high Vacuum
  • 08:07Surface Hydrogen Nuclear Reaction Analysis Measurements
  • 09:24Bulk and Interface Hydrogen Nuclear Reaction Analysis: Preparation and Measurement
  • 11:02Results: Nuclear Reaction Analysis Hydrogen Depth Profiles for Single Crystal Palladium and from Silicon Dioxide Films on Silicon
  • 12:50Conclusion

Summary

Automatic Translation

Automatic Translation

We illustrate the application of 1H(15N,αγ)12C resonant nuclear reaction analysis (NRA) to quantitatively evaluate the density of hydrogen atoms on the surface, in the volume, and at an interfacial layer of solid materials. The near-surface hydrogen depth profiling of a Pd(110) single crystal and of SiO2/Si(100) stacks is described.

Tags

Hydrogen ConcentrationNuclear Reaction AnalysisDepth ProfilingSurface And Interface LayersBulk MaterialsHydrogen StorageFuel CellsHydrogenation CatalystsSemiconductor TechnologyPalladiumLow Energy Electron DiffractionAuger Electron Spectroscopy

Article

Embed

ADD TO PLAYLIST

Usage Statistics

Related Videos

check_url/53452?article_type=v

Controlling the Size, Shape and Stability of Supramolecular Polymers in Water
check_url/53452?article_type=v

Printing Fabrication of Bulk Heterojunction Solar Cells and In Situ Morphology Characterization
check_url/53452?article_type=v

Fabrication and Operation of Acoustofluidic Devices Supporting Bulk Acoustic Standing Waves for Sheathless Focusing of Particles
check_url/53452?article_type=v

Simultaneous Multi-surface Anodizations and Stair-like Reverse Biases Detachment of Anodic Aluminum Oxides in Sulfuric and Oxalic Acid Electrolyte
check_url/53452?article_type=v

In Situ High Pressure Hydrogen Tribological Testing of Common Polymer Materials Used in the Hydrogen Delivery Infrastructure
check_url/53452?article_type=v

Processing of Bulk Nanocrystalline Metals at the US Army Research Laboratory
check_url/53452?article_type=v

Methods of Ex Situ and In Situ Investigations of Structural Transformations: The Case of Crystallization of Metallic Glasses
check_url/53452?article_type=v

Bulk and Thin Film Synthesis of Compositionally Variant Entropy-stabilized Oxides
check_url/53452?article_type=v

Determining Tribocorrosion Rate and Wear-Corrosion Synergy of Bulk and Thin Film Aluminum Alloys
check_url/53452?article_type=v

Theoretical Calculation and Experimental Verification for Dislocation Reduction in Germanium Epitaxial Layers with Semicylindrical Voids on Silicon

Read Article