Journal
/
Environment
/
Chemical Analysis of Water-accommodated Fractions of Crude Oil Spills Using TIMS-FT-ICR MS
JoVE Journal
Environment
A subscription to JoVE is required to view this content.  Sign in or start your free trial.
JoVE Journal Environment
Chemical Analysis of Water-accommodated Fractions of Crude Oil Spills Using TIMS-FT-ICR MS

Chemical Analysis of Water-accommodated Fractions of Crude Oil Spills Using TIMS-FT-ICR MS

DOI:
10.3791/55352-v

•

08:17 min

•

March 03, 2017

•

, , , ,
1Chemistry and Biochemistry,Florida International University

Chapters

  • 00:05Title
  • 01:07Low-energy Water-accommodated Fraction (LEWAF) Sample Preparation and Photoirradiation
  • 03:37Fourier Transform–Ion Cyclotron Resonance Mass Spectrometry (FT-ICR MS) and Trapped Ion Mobility Spectrometry (TIMS) with Atmospheric Pressure Laser Ionization (APLI)
  • 05:47Results: Analysis of LEWAF Composition by TIMS-FT-ICR MS with APLI
  • 06:45Conclusion

Summary

Automatic Translation

Automatic Translation

The low-energy water-accommodated fraction (LEWAF) of crude oil is a challenging system to analyze, because over time, this complex mixture undergoes chemical transformations. This protocol illustrates methods for the preparation of the LEWAF sample and for performing photo-irradiation and chemical analysis by trapped ion mobility spectrometry–FT-ICR MS.

Tags

Keywords: Chemical AnalysisWater-accommodated FractionsCrude Oil SpillsTIMS-FT-ICR MSMolecular CharacterizationComplex MixturesMobility Resolving PowersMass ResolutionMass AccuracyLEGAF PreparationArtificial SeawaterCrude Oil SampleLEWAFSolar IrradiatorDichloromethane Extraction

Article

Embed

ADD TO PLAYLIST

Usage Statistics

Related Videos

check_url/55352?article_type=v

Measurement of H2S in Crude Oil and Crude Oil Headspace Using Multidimensional Gas Chromatography, Deans Switching and Sulfur-selective Detection
check_url/55352?article_type=v

LC-MS Analysis of Human Platelets as a Platform for Studying Mitochondrial Metabolism
check_url/55352?article_type=v

Methods of Soil Resampling to Monitor Changes in the Chemical Concentrations of Forest Soils
check_url/55352?article_type=v

Measurement of the Rheology of Crude Oil in Equilibrium with CO2 at Reservoir Conditions
check_url/55352?article_type=v

Dispersion of Nanomaterials in Aqueous Media: Towards Protocol Optimization
check_url/55352?article_type=v

Microfluidic Devices for Characterizing Pore-scale Event Processes in Porous Media for Oil Recovery Applications
check_url/55352?article_type=v

The Effect of the Application of Thyme Essential Oil on Microbial Load During Meat Drying
check_url/55352?article_type=v

Identification of Pharmaceuticals in The Aquatic Environment Using HPLC-ESI-Q-TOF-MS and Elimination of Erythromycin Through Photo-Induced Degradation
check_url/55352?article_type=v

A Novel Method for the Pentosan Analysis Present in Jute Biomass and Its Conversion into Sugar Monomers Using Acidic Ionic Liquid
check_url/55352?article_type=v

Isolation of Mandibular Gland Reservoir Contents from Bornean ‘Exploding Ants’ (Formicidae) for Volatilome Analysis by GC-MS and MetaboliteDetector

Read Article