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Nitrogen Compound Characterization in Fuels by Multidimensional Gas Chromatography
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JoVE Journal Chemistry
Nitrogen Compound Characterization in Fuels by Multidimensional Gas Chromatography

Nitrogen Compound Characterization in Fuels by Multidimensional Gas Chromatography

DOI:
10.3791/60883-v

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08:22 min

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May 15, 2020

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, , , ,
1U.S. Naval Research Laboratory, 2NRC Research Associateships Programs, 3Nova Research, Inc., 4Peraton, 5Naval Air Systems Command, Air-4.4.5.

Chapters

  • 00:04Introduction
  • 00:42Calibration Standard Preparation and Column Installation
  • 02:18Method Parameter Setup
  • 03:11Instrument Calibration
  • 04:17Sample Analysis
  • 04:55Data Analysis
  • 06:01Results: Representative Two-Dimensional Gas Chromatography and Nitrogen Chemiluminescence Detection (GCxGC-NCD) Chromatograms
  • 07:38Conclusion

Summary

Automatic Translation

Automatic Translation

Here, we present a method utilizing two-dimensional gas chromatography and nitrogen chemiluminescence detection (GCxGC-NCD) to extensively characterize the different classes of nitrogen-containing compounds in diesel and jet fuels.

Tags

Keywords: Nitrogen Compound CharacterizationFuelsMultidimensional Gas ChromatographyJet FuelDiesel FuelCompound Class-level InformationNitrogen DistributionFuel BehaviorFuel PerformanceCost-efficient InstrumentationQuantitationSample PreparationSecondary GC ColumnModulatorColumn InstallationCalibration StandardsGas Chromatography VialsPrimary ColumnSplitless InletSecondary ColumnWite-Out PenMicro-unionNitrogen Chemiluminescence DetectionInstrument ParametersOven TemperatureRamp RateHot Jet TemperatureLiquid Nitrogen Dewar

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