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Synthesis and Performance Characterizations of Transition Metal Single Atom Catalyst for Electrochemical CO2 Reduction
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Journal JoVE Chimie
Synthesis and Performance Characterizations of Transition Metal Single Atom Catalyst for Electrochemical CO2 Reduction

Synthesis and Performance Characterizations of Transition Metal Single Atom Catalyst for Electrochemical CO2 Reduction

DOI:
10.3791/57380-v

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10:57 min

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April 10, 2018

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, ,
1Rowland Institute,Harvard University, 2Materials Science and Engineering,Stanford University

Chapitres

  • 00:05Titre
  • 00:44Preparation of Ni Single-atom Catalyst (NiN-GS)
  • 03:57Electrochemical CO2 Reduction Measurements
  • 07:03CO2 Reduction Product Analysis by Gas Chromatography
  • 08:58Results: Characterization and Electrocatalytic Performance of NiN-GS
  • 10:30Conclusion

Summary

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Here, we present a protocol for the synthesis and electrochemical testing of transition metal single atoms coordinated in graphene vacancies as active centers for selective carbon dioxide reduction to carbon monoxide in aqueous solutions.

Tags

Transition MetalSingle Atom CatalystElectrochemical CO2 ReductionGraphene VacanciesPolyacrylonitrilePolyvinylpyrrolidoneNickel(II)hexahydrateDicyandiamideElectrospinningCarbon Fiber PaperPolymer Nano-fiber Film

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