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트리카보닐(트로폰)철을 통한 6-아미노사이클로헵타-2,4-디엔-1-1-1 유도체 의 제조
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Chimie
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Journal JoVE Chimie
Preparation of 6-aminocyclohepta-2,4-dien-1-one Derivatives via Tricarbonyl(tropone)iron
DOI:

07:56 min

August 12, 2019

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Chapitres

  • 00:04Titre
  • 00:28Synthesis of Aza-Michael Adduct 4: Tricarbonyl[(2-5-η)-6-((2-phenylethyl) Amino cyclohepta-2,4-dien-1-one]Iron
  • 01:48Synthesis of Tricarbonyl[(2-5-η)-6-(2-methylanilino)cyclohepta-2, 4-dien-1-one]Iron (3)
  • 02:55Protection of Amine 4 as a Tert-butyl Carbamate
  • 04:30Synthesis of Tert-butyl (6-oxocyclohepta-2, 4-dien-1-yl)(2-phenylethyl) Carbamate (6)
  • 05:41Results: Description of NMR Spectral Data for Selected Compounds
  • 07:17Conclusion

Summary

Traduction automatique

삼보손(tropone) 철에 아민 핵소를 첨가하기 위한 대표적인 실험 절차와 생성된 복합체의 후속 탈환이 상세히 제시된다.

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