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Journal
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Chemistry
/
A Protocol for Safe Lithiation Reactions Using Organolithium Reagents
JoVE Journal
Chemistry
This content is Free Access.
JoVE Journal
Chemistry
A Protocol for Safe Lithiation Reactions Using Organolithium Reagents
A Protocol for Safe Lithiation Reactions Using Organolithium Reagents
DOI:
10.3791/54705-v
•
09:45 min
•
November 12, 2016
•
Michael R. Gau
,
Michael J. Zdilla
1
Department of Chemistry
,
Temple University
Chapters
00:05
Title
00:39
Organolithium Handling and Disposal Procedures
02:07
Small-scale Lithiation
06:21
Lithiation in a Glovebox
08:25
Results: Lithiation of
tert
-Butylamine with
tert
-Butyllithium
08:54
Conclusion
Summary
Automatic Translation
English (Original)
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Automatic Translation
The safe and proper use of organolithium reagents is described.
Tags
Organolithium Reagents
Lithiation Reactions
Safety Protocol
Pyrophoric Reagents
Synthetic Chemistry
Quenching Agents
Inert Gas Blanket
Schlenk Flask
Tert-butylamine
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