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Chapters
- 00:05Title
- 02:21Preparation of [RuII(PhTpy)(5,5′-dybpy)(MeCN)](PF6)2 Monomer Solution in Electrolyte Solution
- 03:25Electropolymerization of [RuII(PhTpy)(5,5′-dybpy)(MeCN)](PF6)2
- 05:58Surface Coverage Determination
- 07:04Results: Vinyl-based Reductive Electropolymerization of Poly-pyridyl Complexes
- 08:17Conclusion
A procedure for performing reductive electropolymerization of vinyl-containing compounds onto glassy carbon and fluorine doped tin-oxide coated electrodes is presented. Recommendations on electrochemical cell configurations and troubleshooting procedures are included. Although not explicitly described here, oxidative electropolymerization of pyrrole-containing compounds follows similar procedures to vinyl-based reductive electropolymerization.
