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Chapters
- 00:05Title
- 01:04Preparation of Solvents and Solutions
- 02:08High-temperature Solid-state Reactions
- 04:04In Situ Reduction and Solvothermal Reactions
- 06:00Reactive Layering
- 07:20Results: Synthesis and Characterization of Chalcogenidoplumbates
- 09:28Conclusion
The synthesis of chalcogenidoplumbates(II,IV) via the in situ reduction of nominal "PbCh2" (Ch = Chalcogen) and via a solid-state reaction and subsequent solvothermal reactions is presented. Additionally, reactivities of plumbate(II) solutions are portrayed, which yield the heaviest-known CO homolog known to date: the µ-PbSe ligand.
