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Methods of Ex Situ and In Situ Investigations of Structural Transformations
 

Methods of Ex Situ and In Situ Investigations of Structural Transformations: The Case of Crystallization of Metallic Glasses

Article DOI: 10.3791/57657-v 08:55 min June 7th, 2018
June 7th, 2018

챕터

요약

Here, we present a protocol to describe ex situ and in situ investigations of structural transformations in metallic glasses. We employed nuclear-based analytical methods which inspect hyperfine interactions. We demonstrate the applicability of Mössbauer spectrometry and nuclear forward scattering of synchrotron radiation during temperature-driven experiments.

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Keywords: Ex Situ In Situ Structural Transformations Crystallization Metallic Glasses Mössbauer Spectroscopy Nuclear Forward Scattering Synchrotron Radiation X-ray Diffraction DSC Annealing Amorphous Iron-based Magnetic Microstructure Hyperfine Interactions
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