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小分子的微晶电子衍射
JoVE Journal
Biochemistry
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JoVE Journal Biochemistry
Microcrystal Electron Diffraction of Small Molecules
DOI:

09:48 min

March 15, 2021

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Chapters

  • 00:04Introduction
  • 00:34Preparing Small Molecule Samples and TEM Grids
  • 01:37Applying Sample to Grids by Creating a Homogenous Fine Powder
  • 02:51Freezing and Loading Grids into the TEM
  • 04:12Locating and Screening Nanocrystals
  • 07:33Collecting MicroED Data
  • 08:36Results: Analysis of MicroED Dataset from Carbamazepine Microcrystal
  • 09:10Conclusion

Summary

Automatic Translation

在这里,我们描述了我们实验室开发的用于制备用于微晶电子衍射(MicroED)实验的小分子晶体粉末的程序。

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