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连续流反应器中的可扩展巴尔茨-席曼反应方案
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JoVE Journal
Chemistry
A Scalable Balz-Schiemann Reaction Protocol in a Continuous Flow Reactor
Please note that all translations are automatically generated.
Click here for the English version.
连续流反应器中的可扩展巴尔茨-席曼反应方案
DOI:
10.3791/64937-v
•
05:21 min
•
February 10, 2023
•
Zhangtao Zhou
2
,
Yang Wang
,
Shuqiang Liu
,
Andrew Phillis
2
,
Qijun Zhang
,
Weiping Ye
1
Shenzhen Hwagen Pharmaceutical Co., Ltd
,
2
Guangdong Raffles Pharmaceutical Technology Co., Ltd
Chapters
00:04
Introduction
00:46
Continuous Flow Equipment Setup, Safety Check, and Leak Test
02:29
Continuous Flow Reaction Process
03:29
Results: Effect of Temperature and Residence Time on Continuous Flow Reaction
04:33
Conclusion
Summary
Automatic Translation
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Automatic Translation
提出了一个详细的可扩展连续流动方案,用于通过Balz-Schiemann反应从芳基胺合成芳基氟化物。
Tags
Balz-Schiemann Reaction
Continuous Flow Reactor
Aryl Fluoride
Aryl Amine
Fine Chemical Industry
Pharmaceutical Industry
Microflow Reactor
Dynamic Mixing Tube Reactor
Temperature Regulation
Safety
Leakage Check
Steady State Equilibrium
Product Collection
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