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JoVE Journal Chemistry
HKUST-1 as a Heterogeneous Catalyst for the Synthesis of Vanillin
 

HKUST-1 as a Heterogeneous Catalyst for the Synthesis of Vanillin

Article DOI: 10.3791/54054-v • 11:15 min • July 23rd, 2016
July 23rd, 2016 •
1, 1, 1, 2, 3, 4, 5, 5, 1
1Autonomous Metropolitan University-Azcapotzalco, 2Institute of Catalysis and Petroleum Chemistry, ICP-CSIC, 3Department of Chemistry, Autonomous Metropolitan University-Iztapalapa, 4Department of Chemistry, Center of Investigation and Superior Studies (IPN), 5Research Institute of Material, National Autonomous University of Mexico

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요약
Automatic Translation

The conversion of trans-ferulic acid to vanillin was achieved by heterogeneous catalysis. HKUST-1 was employed in this synthesis and the essential step in the catalytic process was the generation of unsaturated metal sites. Thus, when the catalyst was activated under vacuum, full vanillin conversion (yield of 95%) was obtained.

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Keywords: HKUST-1 Heterogeneous Catalyst Vanillin Synthesis Ferulic Acid Conversion Porous Coordination Polymer Catalytic Activation Powder X-ray Diffraction Vacuum Activation System
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