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(2<em>ž</em>,4<em>电子</em>) - 通过电子缺陷烯烃与烯丙基乙酸酯的烯化反应制备二烯酰胺
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JoVE Journal
Chemistry
Facile Preparation of (2
Z
,4
E
)-Dienamides by the Olefination of Electron-deficient Alkenes with Allyl Acetate
Please note that all translations are automatically generated.
Click here for the English version.
(2<em>ž</em>,4<em>电子</em>) - 通过电子缺陷烯烃与烯丙基乙酸酯的烯化反应制备二烯酰胺
DOI:
10.3791/55766-v
•
06:46 min
•
June 21, 2017
•
Liyuan Ding
,
Chunbing Yu
,
Zhenqiang Zhao
,
Feifei Li
,
Jian Zhang
,
Guofu Zhong
1
College of Materials, Chemistry and Chemical Engineering
,
Hangzhou Normal University
,
2
Shijiazhuang Mechanized Infantry Academy
Chapters
00:05
Title
01:00
Preparation of Butadienes by the Olefination of Acrylamides with Allyl Acetate
03:41
Results: Preparation of 1,3-Butadiene via Ruthenium-catalyzed Olefination of Acrylamides with Allyl Acetate
05:28
Conclusion
Summary
Automatic Translation
English (Original)
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Automatic Translation
这里描述了电子缺乏烯烃与乙酸烯丙酯的钌催化烯化反应。通过使用氨基羰基作为引导基团,该外部无氧化剂方案具有高效率和良好的立体选择性和开放的新的合成途径(
Z
,
E
) - 丁二烯骨架。
Tags
Olefination
Electron-deficient Alkenes
Allyl Acetate
Ruthenium Catalyst
Z
E-butadienes
Acrylamide
Cross-coupling
Column Chromatography
NMR Spectroscopy
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