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Chemistry
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通过三碳基(特罗酮)铁制备6-氨基环丙烯-2,4-dien-1-1衍生物
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JoVE Journal
Chemistry
Preparation of 6-aminocyclohepta-2,4-dien-1-one Derivatives via Tricarbonyl(tropone)iron
Please note that all translations are automatically generated.
Click here for the English version.
通过三碳基(特罗酮)铁制备6-氨基环丙烯-2,4-dien-1-1衍生物
DOI:
10.3791/60050-v
•
07:56 min
•
August 12, 2019
•
Zhiyuan Huang
,
Zaki K. Phelan
,
Rachel L. Tritt
,
Shelby D. Valent
,
Ziyang Guan
,
Yiqun He
,
Philip S. Weiss
,
Daniel R. Griffith
1
Department of Chemistry
,
Lafayette College
Chapters
00:04
Title
00:28
Synthesis of Aza-Michael Adduct 4: Tricarbonyl[(2-5-η)-6-((2-phenylethyl) Amino cyclohepta-2,4-dien-1-one]Iron
01:48
Synthesis of Tricarbonyl[(2-5-η)-6-(2-methylanilino)cyclohepta-2, 4-dien-1-one]Iron (3)
02:55
Protection of Amine 4 as a Tert-butyl Carbamate
04:30
Synthesis of Tert-butyl (6-oxocyclohepta-2, 4-dien-1-yl)(2-phenylethyl) Carbamate (6)
05:41
Results: Description of NMR Spectral Data for Selected Compounds
07:17
Conclusion
Summary
Automatic Translation
English (Original)
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Automatic Translation
详细介绍了在三碳基(特罗酮)铁中添加胺核亲子的代表性实验程序以及随后产生的复合物的脱金属化。
Tags
Keywords: 6-aminocyclohepta-2
4-dien-1-one
Tropone Derivatives
Aza-Micheal Addition
Aminated Tropone
Synthetic Intermediates
Solvent-free Process
Chromatography
Alumina
Phenylethylamine
O-toluidene
Boc Protection
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